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NJ Low Level TO-15 75 Component Mix on Rtx-VMS (30 m, 2.0 mL/min)
Peaks tR (min)
1. Propylene 1.21
2. Dichlorodifluoromethane (Freon 12) 1.25
3. 1,2-Dichlorotetrafluoroethane (Freon 114) 1.37
4. Chloromethane 1.43
5. n- Butane1.45
6. Vinyl chloride 1.49
7. 1,3-Butadiene 1.51
8. Bromomethane 1.82
9. Chloroethane 1.94
10. Vinyl bromide 2.06
11. n- Pentane2.08
12. Trichlorofluoromethane (Freon 11) 2.09
13. Carbon disulfide 2.64
14. 1,1-Dichloroethene 2.64
15. 1,1,2-Trichlorotrifluoroethane (Freon 113) 2.68
16. Ethanol 2.68
17. Acrolein 3.09
18. Allyl chloride 3.25
19. Methylene chloride 3.40
20. Isopropyl alcohol 3.45
21. Acetone 3.51
22. trans- 1,2-Dichloroethene3.62
23. Hexane 3.75
24. Methyl tert- butyl ether (MTBE) 3.82
25. Tertiary butanol 4.13
26. 1,1-Dichloroethane 4.58
27. Vinyl acetate 5.16
28. cis- 1,2-Dichloroethene5.56
29. Cyclohexane 5.83
30. Bromochloromethane (IS) 5.90
31. Chloroform 6.12
32. Carbon tetrachloride 6.22
33. Tetrahydrofuran 6.36
34. 1,1,1-Trichloroethane 6.37
35. Ethyl acetate 6.46
36. 2-Butanone (MEK) 6.70
37. 2,2,4-Trimethylpentane 6.84
38. Benzene 7.03
39. Heptane 7.07
Peaks tR (min)
40. 1,2-Dichloroethane 7.40
41. Trichloroethylene 8.05
42. 1,4-Difluorobenzene (IS) 8.18
43. 1,2-Dichloropropane 8.90
44. Bromodichloromethane 9.07
45. 1,4-Dioxane 9.44
46. Methyl methacrylate 9.45
47. cis- 1,3-Dichloropropene10.11
48. Toluene 10.46
49. Tetrachloroethene 11.05
50. 4-Methyl-2-pentanone (MIBK) 11.19
51. trans- 1,3-Dichloropropene11.21
52. 1,1,2-Trichloroethane 11.45
53. Dibromochloromethane 11.70
54. 1,2-Dibromoethane 12.01
55. 2-Hexanone (MBK) 12.58
56. Chlorobenzene-d5 (IS) 12.89
57. Chlorobenzene 12.91
58. n- Nonane12.99
59. Ethylbenzene 13.02
60. m- Xylene13.27
61. p- Xylene13.27
62. o- Xylene13.97
63. Bromoform 14.05
64. Styrene 14.07
65. Cumene 14.53
66. 4-Bromofluorobenzene* 14.96
67. n- Propylbenzene15.24
68. 1,1,2,2-Tetrachloroethane 15.42
69. 2-Chlorotoluene 15.44
70. 4-Ethyltoluene 15.45
71. 1,3,5-Trimethylbenzene 15.62
72. 1,2,4-Trimethylbenzene 16.28
73. 1,3-Dichlorobenzene 16.74
74. 1,4-Dichlorobenzene 16.92
75. Benzyl chloride 17.41
76. 1,2-Dichlorobenzene 17.64
77. 1,2,4-Trichlorobenzene 20.28
78. Hexachlorobutadiene 20.29
79. Naphthalene 20.72
*Tuning standard
GC_AR1165
Rtx-VMS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 19915) with MXT low-dead-volume connector kit (cat.# 20536) TO-14A internal standard/tuning mix (cat.# 34408) 75 comp TO15 + NJ mix (cat.# 34396)
Nitrogen 10.0 ppbv 250 mL injection on-column 32 °C (hold 5 min) to 150 °C at 8 °C/min to 230 °C at 33 °C/min He, constant flow 2.0 mL/min 51.15 cm/sec @ 35 °C MS Scan Group Start Time (min) Scan Range (amu) Scan Rate (scans/sec) 1 0.00 35.0 - 226.00 3.8
250 °C Quadrupole Extractor 6 mm ID 230 °C 150 °C 70.0 eV BFB EI Markes CIA Advantage Agilent 7890B GC & 5977A MSD
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