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Organophosphorus Pesticides U.S. EPA Method 8141A on Rtx-OPPesticides2

GC_EV00602
Column | Rtx-OPPesticides2, 30 m, 0.25 mm ID, 0.25 µm (cat.# 11243) |
Sample | Triphenylphosphate (cat.# 32281) |
Tributylphosphate (cat.# 32280) | |
8140/8141 OP pesticide calibration mix A (cat.# 32277) | |
8141 OP pesticide calibration mix B (cat.# 32278) | |
Conc.: | 100 ppm (100 ng on-column) |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.4 min) |
Liner: | Double taper splitless (4 mm) (cat.# 20785) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 80 °C (hold 0.5 min) to 140 °C at 20 °C/min to 210 °C at 4 °C/min (hold 1 min) to 280 °C at 30 °C/min (hold 5 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.0 mL/min |
Detector | MS |
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Analyzer Type: | Quadrupole |
Ionization Mode: | EI |
Scan Range: | 35-400 amu |
Notes | U.S. EPA Method 8141A custom standard mix. Additional mixes not shown. Contact Restek for more information. |
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