500pg of Derivatized Organo Tin Compounds Separated Well on Rtx-5 and Rtx-35 Columns Using GC/FPD.
Peaks | |
---|---|
1. | Tetrapropyltin![]() |
2. | Tetrabutyltin![]() |
3. | Tributyltin |
4. | Dibutyltin![]() |
5. | Tripentyltin |
6. | Monobutyltin |

GC_EV00787
Columns | Rtx-5 30 m, 0.32 mm ID, 1.00 µm (cat.# 10254) |
and Rtx-35 30 m, 0.32 mm ID, 1.00 µm (cat.# 10454) | |
Sample | Derivatized Organo Tin Compounds |
Conc.: | 500 pg on column |
Injection | |
Inj. Vol.: | 3.0 µL Direct |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 100 °C (hold 1 min) to 285 °C at 10 °C/min (hold 10 min) |
Carrier Gas | He, constant pressure (15 psi, 103.4 kPa) |
Detector | FPD @ 250 °C |
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