share:

Volatile Organics US EPA CLP 04.1 on Rtx-VMS

Peaks
1.Dichlorodifluoromethane
2.Chloromethane
3.Vinyl chloride
4.Bromomethane
5.Chloroethane
6.Trichlorofluoromethane
7.1,1-Dichloroethene
8.Carbon disulfide
9.1,1,2-Trichloro-1,2,2-Trifluoroethane
10.Methylene Chloride
11.Acetone
12.trans-1,2-Dichloroethene
13.Methyl acetate
14.Methyl tert-butyl ether
15.1,1-Dichloroethane
16.cis-1,2-dichoroethane
17.Cyclohexane
18.Bromochloromethane (IS)
19.Chloroform
20.Carbon Tetrachloride
21.1,1,1-Trichloroethane
22.2-Butanone
23.Benzene
24.1,2-dichloroethane-d4 (SS)
25.1,2-Dichloroethane
26.Methylcyclohexane
27.Trichloroethene
28.1,4-Difluorobenzene (IS)
Peaks
29.1,2-Dichloropropane
30.Bromodichloromethane
31.cis-1,3-Dichloropropene
32.toluene d8 (SS)
33.Toluene
34.Tetrachloroethane
35.4-Methyl-2-pentanone
36.trans-1,3-dichloropropane
37.1,1,2-Trichloroethane
38.Dibromochloromethane
39.1,2-Dibromoethane
40.2-Hexanone
41.chlorobenzene d5 (IS)
42.Chlorobenzene
43.Ethylbenzene
44.m-Xylene
45.p-Xylene
46.o-Xylene
47.Styrene
48.Bromoform
49.Isopropylbenzene
50.4-Bromofluorobenzene (SS)
51.1,1,2,2-Tetrachloroethane
52.1,3-Dichlorobenzene
53.1,4-Dichlorobenzene
54.1,2-Dichlorobenzene
55.1,2-Dibromo-3-Chloropropane
56.1,2,4-Trichlorobenzene
image
GC_EV00812
ColumnRtx -VMS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 19915)
SampleCLP 04.1 VOA CAL2000 MegaMix, 2000μg/mL in methanol (cat.# 30456)
502.2 Calibration Mix #1 (gases), 2000μg/mL in methanol (cat.# 30042)
VOA Calibration Mix #1 (ketones), 5000μg/mL in methanol/water (90:10) (cat.# 30006)
VOA Internal Standard Mix, 2500μg/mL in methanol (cat.# 30011)
VOA Surrogate Spike Mix, 2500ug/mL in methanol (cat.# 30004)
Diluent:25mL water
Conc.: 20 ppb each analyte, ketones 100 ppb each
Injectionpurge and trap split (split ratio 35:1)
Liner:1mm Split (cat.# 20972-214.1)
Inj. Temp.:200 °C
Purge and Trap
Instrument:OI 4660 Eclipse Purge and Trap
Trap Type:#10 (Tenax/silica gel/carbon molecular sieve)
Purge: 11 min, flow 40 mL/min
Desorb Preheat Temp.:185 °C
Desorb: 0.5 min @ 190 °C, flow 35 mL/min
Bake: 8 min @ 210 °C
Interface Connection:injection port
Transfer Line Temp.:150 °C
Oven
Oven Temp.:40 °C (hold 4 min) to 90 °C at 16 °C/min to 220 °C at 32 °C/min (hold 5 min)
Carrier GasHe, constant flow
Linear Velocity:34 cm/sec @ 40 °C
DetectorMS
Mode:Scan
Transfer Line Temp.:150 °C
Ionization Mode:EI
Scan Range:35-300 amu
Download PDF

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us