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Pesticides and Brominated Flame Retardants by EPA Method 527 on Rxi-5Sil MS

GC_EV1206
Column | Rxi-5Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 13620) |
using IP Deactivated Guard Column 5 m, 0.53 mm ID (cat.# 10045) | |
with Universal Press-Tight Connectors (cat.# 20429) | |
Sample | PBDE Mix (cat.# 33098) |
Pesticides Mix #1, Method 527 (cat.# 33007) | |
Pesticides Mix #2, Method 527 (cat.# 33008) | |
Internal Standard, Method 527 (cat.# 33010) | |
Surrogate Standard, Method 527 (cat.# 33009) | |
Diluent: | Ethyl acetate:methylene chloride (1:1) |
Conc.: | 40 pg/µL (500 pg on-column) |
Injection | |
Inj. Vol.: | 12.5 µL splitless (hold 0.583 min) |
Liner: | Gooseneck Splitless (4mm) w/Semivolatiles Wool (cat.# 20799-231.5) |
Inj. Temp.: | 250 °C |
Purge Flow: | 40 mL/min |
Oven | |
Oven Temp.: | 40 °C (hold 0.60 min) to 320 °C at 30 °C/min (hold 1.07 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 2 mL/min |
Detector | MS |
Mode: | |
Transfer Line Temp.: | 290 °C |
Analyzer Type: | TOF |
Source Temp.: | 225 °C |
Electron Energy: | -70 eV |
Mass Defect: | -20 mu/100 u |
Solvent Delay Time: | 3.33 min |
Acquisition Range: | 45 - 750 amu |
Spectral Acquisition Rate: | 10 spectra/sec |
Instrument | LECO Pegasus 4D GCxGC-TOFMS |
Notes | Carrier Gas Flow: 2 mL/min. corrected constant flow via pressure ramps |
RELATED CHROMATOGRAM LIBRARY SEARCHES
EPA 527
,EPA method 527
,brominated flame retardants
,drinking water
,pesticides
,LVSI
,large volume splitless injecti
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