share:

This chromatogram may contain analytes that are synonyms of your search terms.

0.5 ng Semivolatile Organics with Appendix IX on Rxi-5Sil MS by U.S. EPA Method 8270

Peaks
1.1,4-Dioxane-d8 (IS)
2.1,4-Dioxane
3.N-Nitrosodimethylamine
4.Pyridine
5.Ethyl methacrylate
6.2-Picoline
7.N-Nitrosomethylethylamine
8.Methyl methanesulfonate
9.2-Fluorophenol (SS)
10.N-Nitrosodiethylamine
11.Ethyl methanesulfonate
12.Benzaldehyde
13.Phenol-d6 (SS)
14.Phenol
15.Aniline
16.Bis(2-chloroethyl) ether
17.Pentachloroethane
18.2-Chlorophenol
19.1,3-Dichlorobenzene
20.1,4-Dichlorobenzene-D4 (IS)
21.1,4-Dichlorobenzene
22.Benzyl alcohol
23.1,2-Dichlorobenzene
24.2-Methylphenol
25.Bis(2-Chloroisopropyl)ether
26.N-Nitrosopyrrolidine
27.3-Methylphenol
28.4-Methylphenol
29.Acetophenone
30.N-Nitrosodipropylamine
31.4-Nitrosomorpholine
32.o-Toluidine
33.Hexachloroethane
34.Nitrobenzene-D5 (SS)
35.Nitrobenzene
36.N-Nitrosopiperidine
37.Isophorone
38.2-Nitrophenol
39.2,4-Dimethylphenol
40.Bis(2-chloroethoxy)methane
41.Benzoic acid
42.2,4-Dichlorophenol
43.α,α-Dimethylphenethylamine
44.1,2,4-Trichlorobenzene
45.Naphthalene-D8 (IS)
46.Naphthalene
47.4-Chloroaniline
48.2,6-Dichlorophenol
49.Hexachloropropene
50.Hexachlorobutadiene
51.N-Nitrosobutylamine
52.Caprolactam
53.1,4-Phenylenediamine
54.4-Chloro-3-methylphenol
55.Isosafrole (isomer)
56.2-Methylnaphthalene
57.1-Methylnaphthalene
58.Hexachlorocyclopentadiene
59.1,2,4,5-Tetrachlorobenzene
60.Isosafrole (isomer)
61.2,4,6-Trichlorophenol
62.2,4,5-Trichlorophenol
63.2-Fluorobiphenyl (SS)
64.Safrole
65.Biphenyl
66.2-Chloronaphthalene
67.1-Chloronaphthalene
68.Diphenyl ether
69.2-Nitroaniline
70.1,4-Naphthoquinone
71.1,4-Dinitrobenzene
72.Dimethyl phthalate
Peaks
73.1,3-Dinitrobenzene
74.2,6-Dinitrotoluene
75.1,2-Dinitrobenzene
76.Acenaphthylene
77.3-Nitroaniline
78.Acenaphthene-d10 (IS)
79.Acenaphthene
80.2,4-Dinitrophenol
81.4-Nitrophenol
82.Pentachlorobenzene
83.2,4-Dinitrotoluene
84.Dibenzofuran
85.1-Naphthalamine
86.2,3,5,6-Tetrachlorophenol
87.2,3,4,6-Tetrachlorophenol
88.2-Naphthalamine
89.Diethyl phthalate
90.4-Chlorophenyl phenyl ether
91.Fluorene
92.2-Methyl-5-nitroaniline
93.4-Nitroaniline
94.4,6-Dinitro-2-methylphenol
95.N-nitrosodiphenylamine (as diphenylamine)
96.1,2-Diphenylhydrazine (as azobenzene)
97.2,4,6-Tribromophenol (SS)
98.1,3,5-Trinitrobenzene
99.Diallate
100.Phenacetin
101.4-Bromophenyl phenyl ether
102.Hexachlorobenzene
103.Atrazine
104.4-Aminobiphenyl
105.Pentachlorophenol
106.Pentachloronitrobenzene
107.Propyzamide
108.Phenanthrene-D10 (IS)
109.Phenanthrene
110.Anthracene
111.Carbazole
112.di-n-Butyl phthalate
113.4-Nitroquinoline 1-oxide
114.Methapyriline
115.Isodrin
116.Fluoranthene
117.Benzidine
118.Pyrene-d10 (SS)
119.Pyrene
120.Aramite (isomer)
121.p-Terphenyl-d14 (SS)
122.Aramite (isomer)
123.Dimethylaminoazobenzene
124.Chlorobenzilate
125.3,3'-Dimethylbenzidine
126.Butyl benzyl phthalate
127.Kepone
128.Bis(2-ethylhexyl) adipate
129.2-Acetylaminofluorene
130.3,3'-Dichlorobenzidine
131.Benz[a]anthracene
132.Chrysene-D12 (IS)
133.Bis(2-ethylhexyl)phthalate
134.Chrysene
135.Di-n-octyl phthalate
136.7,12-Dimethylbenzo[a]anthracene
137.Benzo[b]fluoranthene
138.Benzo[k]fluoranthene
139.Benzo[a]pyrene
140.Perylene-D12 (IS)
141.3-Methylcholanthrene
142.Dibenzo[a,j]acridine
143.Indeno[1,2,3-cd]pyrene
144.Dibenz[a,h]anthracene
145.Benzo[ghi]perylene
image
GC_EV1269
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Sample8270 MegaMix (cat.# 31850)
8270 Benzidines mix (cat.# 31852)
Benzoic acid (cat.# 31879)
Revised B/N surrogate mix (cat.# 31888)
Acid surrogate mix (4/89 SOW) (cat.# 31063)
Revised SV internal standard mix (cat.# 31886)
Appendix IX mix #1 (cat.# 31625)
Appendix IX mix #2 (cat.# 31806)
Diluent:Dichloromethane
Conc.:0.5 µg/mL (IS/SS 20 μg/mL)
Injection
Inj. Vol.:1 µL pulsed splitless (hold 0.59 min)
Liner:Premium 4 mm single taper/gooseneck w/wool (cat.# 23303.1)
Inj. Temp.:270 °C
Pulse Pressure:30 psi (206.8kPa)
Pulse Time:0.64 min
Purge Flow:100 mL/min
Oven
Oven Temp.:40 °C (hold 1 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Source Temp.:276 °C
Quad Temp.:150 °C
Electron Energy:70 eV
Solvent Delay Time:2.19 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
Scan Rate:5.36 scans/sec
InstrumentAgilent 7890A GC & 5975C MSD
Notes7890 Siltek-treated EZ Twist Top split/splitless injection port (cat.# 22178)
Flip Seal dual Vespel ring inlet seal (cat.# 23411)
Download PDF

RELATED CHROMATOGRAM LIBRARY SEARCHES

Appendix IX

,

SVOA

,

8270

,

semivolatiles

,

5sil MS

,

RXI

,

rxi-5sil

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.


Restek Domestic Customer Service

Subject

Message

Your Full Name

Your Email

Company Name

Address

Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.

www.restek.com/Contact-Us