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Brominated Flame Retardants on Rtx-1614 After Twelve Loops Were Trimmed Off

PeaksConc.
(ng/mL)
1.BDE 1200
2.BDE 2200
3.BDE 3200
4.BDE 10200
5.BDE 7200
6.BDE 15200
7.BDE 30200
8.BDE 17200
9.BDE 28200
10.Pentabromoethylbenzene (PBEB)200
11.Hexabromobenzene (HBB)200
12.BDE 49400
13.BDE 71400
14.BDE 47400
15.BDE 66400
16.BDE 77400
17.BDE 100400
18.BDE 119400
19.BDE 99400
20.BDE 85400
21.BDE 126400
22.BB-153400
23.BDE 154400
PeaksConc.
(ng/mL)
24.BDE 153400
25.BDE 139400
26.BDE 140400
27.BDE 138400
28.BDE 156400
29.BDE 169400
30.BDE 184800
31.BDE 183800
32.BDE 191800
33.BTBPE400
34.BDE 180800
35.BDE 171800
36.BDE 201800
37.BDE 204800
38.BDE 197800
39.BDE 203800
40.BDE 196800
41.BDE 205800
42.BDE 2082,000
43.BDE 2072,000
44.BDE 2062,000
45.BDE 2092,000
46.DBDPE4,000
image
GC_EV1307
ColumnRtx-1614, 7.9 m, 0.25 mm ID, 0.10 µm (cat.# 10296)
SampleNative PBDEs/BFRs (Wellington Laboratories) (cat.# BFR-PAR)
Diluent:Nonane/toluene
Injection
Inj. Vol.:1.0 µL splitless (hold 1.0 min)
Liner:Premium 4 mm cyclo double taper (cat.# 23310.5)
Inj. Temp.:340 °C
Oven
Oven Temp.:75 °C (hold 0.3 min) to 210 °C at 52 °C/min to 310 °C at 23 °C/min (hold 1.4 min)
Carrier GasHe, constant flow
Flow Rate:1.6 mL/min
DetectorMS
Mode:SIM
Transfer Line Temp.:330 °C
Analyzer Type:Quadrupole
Source Temp.:350 °C
Quad Temp.:200 °C
InstrumentAgilent 7890A GC & 5975C MSD
NotesCat.# 10296 is a 15 m column. Twelve loops were trimmed off the column for a final column length of 7.9 m.
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RELATED CHROMATOGRAM LIBRARY SEARCHES

flame retardants

,

polybrominated diphenyl ethers

,

PBDE

,

BDE

,

column trimming

,

Rtx-1614

,

EPA Method 1614

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