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Semivolatiles on Rtx-5 with 5 m Integra-Guard by EPA Method 8270

Peaks
1.1,4-Dioxane-D8 (IS)
2.1,4-Dioxane
3.Pyridine
4.N-Nitrosodimethylamine
5.Ethyl methacrylate
6.2-Picoline
7.N-Nitrosomethylethylamine
8.Methyl methanesulfonate
9.2-Fluorophenol (SS)
10.N-Nitrosodiethylamine
11.Ethyl methanesulfonate
12.Benzaldehyde
13.Phenol-D6 (SS)
14.Phenol
15.Aniline
16.Pentachloroethane
17.Bis(2-chloroethyl) ether
18.2-Chlorophenol
19.1,3-Dichlorobenzene
20.Dichlorobenzene-D4 (IS)
21.1,4-Dichlorobenzene
22.Benzyl alcohol
23.1,2-Dichlorobenzene
24.2-Methylphenol
25.Bis(2-Chloroisopropyl)ether
26.4-Methylphenol
27.3-Methylphenol
28.Acetophenone
29.Nitrosopyrrolidine
30.N-Nitrosodipropylamine
31.N-Nitrosomorpholine
32.o-Toluidine
33.Hexachloroethane
34.Nitrobenzene-D5 (SS)
35.Nitrobenzene
36.N-Nitrosopiperidine
37.Isophorone
38.2-Nitrophenol
39.2,4-Dimethylphenol
40.Benzoic acid
41.Bis(2-chloroethoxy)methane
42.2,4-Dichlorophenol
43.Phenyl-tert-butylamine (Phentermine)
44.1,2,4-Trichlorobenzene
45.Naphthalene-D8 (IS)
46.Naphthalene
47.4-Chloroaniline
48.2,6-Dichlorophenol
49.Hexachloropropene
50.Hexachlorobutadiene
51.Caprolactam
52.N-Nitroso-N-butylamine
53.1,4-Phenylenediamine
54.4-Chloro-3-methylphenol
55.Isosafrole I
56.2-Methylnaphthalene
57.1-Methylnaphthalene
58.Isosafrole II
59.1,2,4,5-Tetrachlorobenzene
60.Hexachlorocyclopentadiene
61.2,4,6-Trichlorophenol
62.2,4,5-Trichlorophenol
63.2-Fluorobiphenyl (SS)
64.Safrole
65.Biphenyl
66.2-Chloronaphthalene
67.1-Chloronaphthalene
68.Diphenyl ether
69.2-Nitroaniline
70.1,4-Naphthoquinone
71.1,2-Dinitrobenzene
72.Dimethyl phthalate
Peaks
73.1,3-Dinitrobenzene
74.2,6-Dinitrotoluene
75.Acenaphthylene
76.1,4-Dinitrobenzene
77.3-Nitroaniline
78.Acenaphthene-D10 (IS)
79.Acenaphthene
80.2,4-Dinitrophenol
81.4-Nitrophenol
82.Dibenzofuran
83.2,4-Dinitrotoluene
84.Pentachlorobenzene
85.1-Naphthalamine
86.2,3,5,6-Tetrachlorophenol
87.2,3,4,6-Tetrachlorophenol
88.2-Naphthalamine
89.Diethyl Phthalate
90.4-Chlorophenyl phenyl ether
91.Fluorene
92.2-Methyl-5-nitroaniline
93.4-Nitroaniline
94.4,6-Dinitro-2-methylphenol
95.N-nitrosodiphenylamine (as diphenylamine)
96.N,N'-Diphenylhydrazine (as Azobenzene)
97.2,4,6-Tribromophenol (SS)
98.1,3,5-Trinitrobenzene
99.Diallate
100.Phenacetin
101.4-Bromophenyl phenyl ether
102.Atrazine
103.Hexachlorobenzene
104.4-Aminobiphenyl
105.Propyzamide
106.Pentachlorophenol
107.Pentachloronitrobenzene
108.Phenanthrene-D10 (IS)
109.Phenanthrene
110.Anthracene
111.Carbazole
112.di-n-Butyl phthalate
113.4-Nitroquinoline 1-oxide
114.Isodrin
115.Fluoranthene
116.Benzidine
117.Pyrene-D10 (SS)
118.Pyrene
119.Aramite I
120.p-Terphenyl-D14 (SS)
121.Aramite II
122.Dimethylaminoazobenzene
123.Chlorobenzilate
124.3,3'-Dimethylbenzidine
125.Butyl benzyl phthalate
126.Kepone
127.Bis(2-ethylhexyl) adipate
128.2-(Acetylamino)fluorene
129.Benz[a]anthracene
130.3,3'-Dichlorobenzidine
131.Chrysene-D12 (IS)
132.Chrysene
133.Bis(2-ethylhexyl) phthalate
134.Di-n-octyl phthalate
135.Benzo[b]fluoranthene
136.Benzo[k]fluoranthene
137.7,12-Dimethylbenzo[a]anthracene
138.Benzo[a]pyrene
139.Perylene-D12 (IS)
140.3-Methylcholanthrene
141.Dibenz[a,j]acridine
142.Indeno[1,2,3-cd]pyrene
143.Dibenz[a,h]anthracene
144.Benzo[ghi]perylene
image
GC_EV1357
ColumnRtx-5 w/ 5 m Integra-Guard, 30 m, 0.25 mm ID, 0.50 µm (cat.# 10238-124)
SampleRevised SV internal standard mix (cat.# 31886)
Revised B/N surrogate mix (cat.# 31888)
Acid surrogate mix (4/89 SOW) (cat.# 31063)
8270 MegaMix (cat.# 31850)
8270 Benzidines mix (cat.# 31852)
Benzoic acid (cat.# 31879)
Appendix IX mix #1, revised (cat.# 32459)
Appendix IX mix #2 (cat.# 31806)
Diluent:Dichloromethane
Conc.:10 ng/µL (IS and SS at 20 ng/µL)
Injection
Inj. Vol.:1 µL pulsed splitless (hold 0.7 min)
Liner:Premium 4 mm single taper w/wool (cat.# 23303.5)
Inj. Temp.:270 °C
Pulse Pressure:30 psi (206.8kPa)
Pulse Time:0.8 min
Purge Flow:100 mL/min
Oven
Oven Temp.:40 °C (hold 2 min) to 90 °C at 12.5 °C/min to 246 °C at 25 °C/min to 295 °C at 3 °C/min to 325 °C at 6 °C/min (hold 3 min)
Carrier GasHe, constant flow
Flow Rate:2.08 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
13.535-5505.6
Transfer Line Temp.:320 °C
Analyzer Type:Quadrupole
Source Type:Inert
Drawout Plate:9mm ID
Source Temp.:350 °C
Quad Temp.:180 °C
Electron Energy:69.9 eV
Solvent Delay Time:3.5 min
Ionization Mode:EI
InstrumentAgilent 7890A GC & 5975C MSD
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