Florida TRPH Standard on Rxi-1HT (15 m x 0.25 mm x 0.10 µm)

	Peaks	tR (sec)
1.	C8	60.7
2.	C10	118.7
3.	C12	195.2
4.	C14	269.6
5.	C16	337.6
6.	C18	399.2
7.	C20	455.3
8.	C22	507.0

	Peaks	tR (sec)
9.	C24	554.5
10.	C26	598.3
11.	C28	639.7
12.	C30	678.3
13.	C32	714.3
14.	C34	748.3
15.	C36	780.5
16.	C38	811.1
17.	C40	840.2

GC_EV1362

Column	Rxi-1HT, 15 m, 0.25 mm ID, 0.10 µm (cat.# 13950)
Sample	Florida TRPH standard (cat.# 31266)
Diluent:	Hexane
Conc.:	500 ng/µL
Injection
Inj. Vol.:	1 µL split (split ratio 250:1)
Liner:	Premium 4 mm Precision liner w/wool (cat.# 23305.5)
Inj. Temp.:	275 °C
Split Vent Flow Rate:	437.5 mL/min
Oven
Oven Temp.:	40 °C (hold 0.1 min) to 400 °C at 20 °C/min (hold 1.9 min)
Carrier Gas	H2, constant flow
Flow Rate:	1.75 mL/min
Detector	FID @ 420 °C
Constant Column + Constant Make-up:	50 mL/min
Make-up Gas Type:	N2
Hydrogen flow:	40 mL/min
Air flow:	450 mL/min
Data Rate:	20 Hz
Instrument	Agilent/HP6890 GC
Notes	Actual column length was calculated to be 15.7 m using holdup time and EZGC flow calculator (http://www.restek.com/ezgc-mtfc).

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