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Semivolatiles on Rxi-5ms (Split Injection)

PeakstR (min)
1.1,4-Dioxane-D8 (IS) 1.98
2.N-Nitrosodimethylamine2.15
3.Pyridine2.18
4.2-Fluorophenol (SS) 2.87
5.Phenol-D6 (SS) 3.48
6.Phenol3.49
7.Aniline3.54
8.bis-(2-chloroethyl)ether3.57
9.2-Chlorophenol3.62
10.1,3-Dichlorobenzene3.74
11.1,4-Dichlorobenzene-D4 (IS) 3.76
12.1,4-Dichlorobenzene3.77
13.Benzyl Alcohol3.86
14.1,2-Dichlorobenzene3.92
15.2-Methylphenol3.95
16.Bis(2-Chloroisopropyl)ether3.98
17.4-Methylphenol4.06
18.3-Methylphenol4.06
19.N-Nitrosodi-N-propylamine4.09
20.Hexachloroethane4.17
21.Nitrobenzene-D5 (SS) 4.21
22.Nitrobenzene4.22
23.Isophorone4.41
24.2-Nitrophenol4.49
25.2,4-Dimethylphenol4.5
26.Benzoic acid4.54
27.Bis(2-chloroethoxy)methane4.58
28.2,4-Dichlorophenol4.67
29.1,2,4-Trichlorobenzene4.76
30.Naphthalene-D8 (IS) 4.79
31.Naphthalene4.81
32.4-Chloroaniline4.86
33.Hexachlorobutadiene4.96
34.4-Chloro-3-methylphenol5.26
35.2-Methylnaphthalene5.4
36.1-Methylnaphthalene5.49
37.Hexachlorocyclopentadiene5.6
38.2,4,6-Trichlorophenol5.66
39.2,4,5-Trichlorophenol5.69
40.2-Fluorobiphenyl (SS) 5.73
41.2-Chloronaphthalene5.82
42.2-Nitroaniline5.93
43.1,4-Dinitrobenzene6.02
44.Dimethyl phthalate6.11
45.1,3-Dinitrobenzene6.12
46.2,6-Dinitrotoluene6.17
47.Acenaphthylene6.19
PeakstR (min)
48.1,2-Dinitrobenzene6.23
49.3-Nitroaniline6.29
50.Acenaphthene-D10 (IS) 6.33
51.Acenaphthene6.35
52.2,4-Dinitrophenol6.38
53.4-Nitrophenol6.42
54.Dibenzofuran6.49
55.2,4-Dinitrotoluene6.51
56.2,3,5,6-Tetrachlorophenol6.59
57.2,3,4,6-Tetrachlorophenol6.63
58.Diethyl Phthalate6.72
59.4-Chlorophenyl phenyl ether6.79
60.Fluorene6.8
61.4-Nitroaniline6.83
62.4,6-Dinitro-2-methylphenol6.87
63.N-Nitrosodiphenylamine (as Diphenylamine)6.89
64.N,N'-Diphenylhydrazine (as Azobenzene)6.93
65.2,4,6-Tribromophenol (SS) 7.02
66.4-Bromophenyl phenyl ether7.22
67.Hexachlorobenzene7.36
68.Pentachlorophenol7.51
69.Phenanthrene-D10 (IS) 7.62
70.Phenanthrene7.64
71.Anthracene7.68
72.Carbazole7.82
73.di-n-Butyl phthalate8.16
74.Fluoranthene8.73
75.Benzidine8.85
76.Pyrene-D10 (SS) 8.95
77.Pyrene8.97
78.p-Terphenyl-D14 (SS) 9.14
79.3,3'-Dimethylbenzidine9.74
80.Butyl benzyl phthalate9.79
81.Bis(2-ethylhexyl) adipate9.89
82.3,3'-Dichlorobenzidine10.6
83.Benz[a]anthracene10.62
84.Chrysene-D12 (IS) 10.65
85.Chrysene10.69
86.Bis(2-ethylhexyl) phthalate10.8
87.Di-n-octyl phthalate12.14
88.Benzo[b]fluoranthene12.93
89.Benzo[k]fluoranthene12.99
90.Benzo[a]pyrene13.77
91.Perylene-D12 (IS) 13.93
92.Indeno[1,2,3-cd]pyrene16.56
93.Dibenz[a,h]anthracene16.62
94.Benzo[ghi]perylene17
image
GC_EV1418
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleRevised SV internal standard mix (cat.# 31886)
Revised B/N surrogate mix (cat.# 31888)
Acid surrogate mix (4/89 SOW) (cat.# 31063)
8270 MegaMix (cat.# 31850)
8270 Benzidines mix (cat.# 31852)
Benzoic acid (cat.# 31879)
Diluent:Dichloromethane
Conc.:5.0 ng/µL (IS and SS concentrations are 20 ng/µL)
Injection
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Premium 4 mm Precision liner w/wool (cat.# 23305.5)
Inj. Temp.:275 °C
Oven
Oven Temp.:50 °C (hold 0.5 min) to 265 °C at 28 °C/min to 285 °C at 3 °C/min to 330 °C at 20 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.44 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
11.535-5505.4
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Source Type:Extractor
Extractor Lens:9mm ID
Source Temp.:350 °C
Quad Temp.:200 °C
Electron Energy:70 eV
Tune Type:DFTPP
Ionization Mode:EI
InstrumentAgilent 7890B GC & 5977A MSD
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