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Semivolatiles on Rxi-5ms (Split Injection)
Peaks tR (min)
1. 1,4-Dioxane-D8 (IS) 1.98
2. N-Nitrosodimethylamine 2.15
3. Pyridine 2.18
4. 2-Fluorophenol (SS) 2.87
5. Phenol-D6 (SS) 3.48
6. Phenol 3.49
7. Aniline 3.54
8. bis-(2-chloroethyl)ether 3.57
9. 2-Chlorophenol 3.62
10. 1,3-Dichlorobenzene 3.74
11. 1,4-Dichlorobenzene-D4 (IS) 3.76
12. 1,4-Dichlorobenzene 3.77
13. Benzyl Alcohol 3.86
14. 1,2-Dichlorobenzene 3.92
15. 2-Methylphenol 3.95
16. Bis(2-Chloroisopropyl)ether 3.98
17. 4-Methylphenol 4.06
18. 3-Methylphenol 4.06
19. N-Nitrosodi-N-propylamine 4.09
20. Hexachloroethane 4.17
21. Nitrobenzene-D5 (SS) 4.21
22. Nitrobenzene 4.22
23. Isophorone 4.41
24. 2-Nitrophenol 4.49
25. 2,4-Dimethylphenol 4.5
26. Benzoic acid 4.54
27. Bis(2-chloroethoxy)methane 4.58
28. 2,4-Dichlorophenol 4.67
29. 1,2,4-Trichlorobenzene 4.76
30. Naphthalene-D8 (IS) 4.79
31. Naphthalene 4.81
32. 4-Chloroaniline 4.86
33. Hexachlorobutadiene 4.96
34. 4-Chloro-3-methylphenol 5.26
35. 2-Methylnaphthalene 5.4
36. 1-Methylnaphthalene 5.49
37. Hexachlorocyclopentadiene 5.6
38. 2,4,6-Trichlorophenol 5.66
39. 2,4,5-Trichlorophenol 5.69
40. 2-Fluorobiphenyl (SS) 5.73
41. 2-Chloronaphthalene 5.82
42. 2-Nitroaniline 5.93
43. 1,4-Dinitrobenzene 6.02
44. Dimethyl phthalate 6.11
45. 1,3-Dinitrobenzene 6.12
46. 2,6-Dinitrotoluene 6.17
47. Acenaphthylene 6.19
Peaks tR (min)
48. 1,2-Dinitrobenzene 6.23
49. 3-Nitroaniline 6.29
50. Acenaphthene-D10 (IS) 6.33
51. Acenaphthene 6.35
52. 2,4-Dinitrophenol 6.38
53. 4-Nitrophenol 6.42
54. Dibenzofuran 6.49
55. 2,4-Dinitrotoluene 6.51
56. 2,3,5,6-Tetrachlorophenol 6.59
57. 2,3,4,6-Tetrachlorophenol 6.63
58. Diethyl Phthalate 6.72
59. 4-Chlorophenyl phenyl ether 6.79
60. Fluorene 6.8
61. 4-Nitroaniline 6.83
62. 4,6-Dinitro-2-methylphenol 6.87
63. N-Nitrosodiphenylamine (as Diphenylamine) 6.89
64. N,N'-Diphenylhydrazine (as Azobenzene) 6.93
65. 2,4,6-Tribromophenol (SS) 7.02
66. 4-Bromophenyl phenyl ether 7.22
67. Hexachlorobenzene 7.36
68. Pentachlorophenol 7.51
69. Phenanthrene-D10 (IS) 7.62
70. Phenanthrene 7.64
71. Anthracene 7.68
72. Carbazole 7.82
73. di-n- Butyl phthalate 8.16
74. Fluoranthene 8.73
75. Benzidine 8.85
76. Pyrene-D10 (SS) 8.95
77. Pyrene 8.97
78. p- Terphenyl-D14 (SS) 9.14
79. 3,3'-Dimethylbenzidine 9.74
80. Butyl benzyl phthalate 9.79
81. Bis(2-ethylhexyl) adipate 9.89
82. 3,3'-Dichlorobenzidine 10.6
83. Benz[a]anthracene 10.62
84. Chrysene-D12 (IS) 10.65
85. Chrysene 10.69
86. Bis(2-ethylhexyl) phthalate 10.8
87. Di-n- octyl phthalate 12.14
88. Benzo[b]fluoranthene 12.93
89. Benzo[k]fluoranthene 12.99
90. Benzo[a]pyrene 13.77
91. Perylene-D12 (IS) 13.93
92. Indeno[1,2,3-cd]pyrene 16.56
93. Dibenz[a,h]anthracene 16.62
94. Benzo[ghi]perylene 17
GC_EV1418
Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) Revised SV internal standard mix (cat.# 31886) Revised B/N surrogate mix (cat.# 31888) Acid surrogate mix (4/89 SOW) (cat.# 31063) 8270 MegaMix (cat.# 31850) 8270 Benzidines mix (cat.# 31852) Benzoic acid (cat.# 31879)
Dichloromethane 5.0 ng/µL (IS and SS concentrations are 20 ng/µL) 1 µL split (split ratio 10:1) Premium 4 mm Precision liner w/wool (cat.# 23305.5) 275 °C 50 °C (hold 0.5 min) to 265 °C at 28 °C/min to 285 °C at 3 °C/min to 330 °C at 20 °C/min (hold 5 min) He, constant flow 1.44 mL/min MS Scan Group Start Time (min) Scan Range (amu) Scan Rate (scans/sec) 1 1.5 35-550 5.4
280 °C Quadrupole Extractor 9mm ID 350 °C 200 °C 70 eV DFTPP EI Agilent 7890B GC & 5977A MSD
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