EPA Method 525.3 PAH Calibration Standard (with 525.3 Internal and Surrogate Standards) on Rxi-5Sil MS

GC_EV1434
Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) | ||||||||
Sample | EPA Method 525.3 PAH cal standard (cat.# 32545) | ||||||||
EPA Method 525.3 PAH IS mix (cat.# 32547) | |||||||||
EPA Method 525.3 PCP IS (cat.# 32548) | |||||||||
EPA Method 525.3 surrogate standard (cat.# 32549) | |||||||||
Diluent: | Ethyl acetate | ||||||||
Conc.: | 2 µg/mL | ||||||||
Injection | |||||||||
Inj. Vol.: | 1 µL pulsed splitless (hold 1 min) | ||||||||
Liner: | Premium 4 mm single taper w/wool (cat.# 23303.1) | ||||||||
Inj. Temp.: | 275 °C | ||||||||
Pulse Pressure: | 30 psi (206.8kPa) | ||||||||
Pulse Time: | 1 min | ||||||||
Purge Flow: | 80 mL/min | ||||||||
Oven | |||||||||
Oven Temp.: | 70 °C (hold 1 min) to 200 °C at 10 °C/min to 320 °C at 7 °C/min (hold 3 min) | ||||||||
Carrier Gas | He, constant flow | ||||||||
Flow Rate: | 1.2 mL/min | ||||||||
Detector | MS | ||||||||
Mode: | Scan | ||||||||
Scan Program: |
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Transfer Line Temp.: | 280 °C | ||||||||
Analyzer Type: | Quadrupole | ||||||||
Source Type: | Extractor | ||||||||
Extractor Lens: | 6 mm ID | ||||||||
Source Temp.: | 350 °C | ||||||||
Quad Temp.: | 200 °C | ||||||||
Solvent Delay Time: | 5 min | ||||||||
Tune Type: | DFTPP | ||||||||
Ionization Mode: | EI | ||||||||
Instrument | Agilent 7890B GC & 5977A MSD |
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