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EPA Method 525.3 Full Analyte List on Rxi-5Sil MS
Peaks tR (min)
1. Diisopropyl methylphosphonate (DIMP) 5.16
2. Isophorone 6.13
3. 1,3-Dimethyl-2-nitrobenzene (SS) 7.03
4. Dichlorvos 7.80
5. Hexachlorocyclopentadiene (HCCPD) 9.08
6. S-Ethyl dipropylthiocarbamate (EPTC) 9.38
7. Mevinphos I 10.20
8. Mevinphos II 10.25
9. Butylate 10.32
10. Vernolate 10.55
11. Dimethylphthalate 10.58
12. Etridiazole 10.60
13. 2,6-Dinitrotoluene 10.67
14. Pebulate 10.73
15. Acenaphthylene 10.74
16. Acenaphthene-D10 (IS) 11.09
17. 2-Chlorobiphenyl 11.29
18. Butylated hydroxytoluene (BHT) 11.30
19. Chloroneb 11.30
20. Tebuthiuron 11.46
21. 2,4-Dinitrotoluene 11.61
22. Molinate 11.75
23. N,N-Diethyl-meta-toluamide (DEET) 12.14
24. Diethylphthalate 12.28
25. 4-Chlorobiphenyl 12.30
26. Fluorene 12.39
27. Propachlor 12.51
28. Ethoprop 12.83
29. Cycloate 12.87
30. Chlorpropham 13.09
31. Trifluralin 13.17
32. Phorate 13.50
33. α-HCH 13.61
34. 2,4'-Dichlorobiphenyl 13.67
35. Hexachlorobenzene 13.70
36. Atraton 13.88
37. Prometon 14.01
38. Simazine 14.02
39. Dimethipin 14.09
40. Atrazine 14.11
41. β-HCH 14.12
42. Pentachlorophenol-C13 (IS) 14.19
43. Propazine 14.19
44. Pentachlorophenol 14.20
45. γ-HCH (Lindane) 14.33
46. Pronamide 14.49
47. 2,2',5-Trichlorobiphenyl 14.56
48. Phenanthrene-D10 (IS) 14.61
49. Phenanthrene 14.66
50. Chlorothalonil 14.66
51. Terbacil 14.77
52. Disulfoton 14.78
53. Anthracene 14.79
54. δ-HCH 14.90
55. Phosphamidon 15.37
56. Acetochlor 15.55
57. Metribuzin 15.56
58. 2,4,4'-Trichlorobiphenyl 15.61
59. Vinclozolin 15.66
60. Methyl parathion 15.71
61. Alachlor 15.75
62. Simetryn 15.81
63. Ametryn 15.90
64. Heptachlor 15.94
65. Prometryn 15.96
66. Terbutryn 16.25
Peaks tR (min)
67. Bromacil 16.31
68. 2,2',5,5'-Tetrachlorobiphenyl 16.37
69. Dibutyl phthalate 16.40
70. Metolachlor 16.60
71. Chlorpyrifos 16.64
72. Cyanazine 16.70
73. Aldrin 16.76
74. Dacthal (DCPA) 16.77
75. 2,2',3,5'-Tetrachlorobiphenyl 16.81
76. Ethyl parathion 16.81
77. Triadimefon 16.89
78. Diphenamid 17.15
79. MGK 264(a) 17.19
80. MGK 264(b) 17.49
81. Chlorfenvinphos 17.64
82. Heptachlor epoxide 17.65
83. 2,3',4',5-Tetrachlorobiphenyl 17.76
84. trans- Chlordane18.20
85. Tetrachlorvinphos 18.27
86. Butachlor 18.35
87. Pyrene 18.46
88. cis- Chlordane18.51
89. Endosulfan I 18.52
90. trans- Nonachlor18.59
91. Napropamide 18.66
92. Profenofos 18.90
93. 4,4'-DDE 19.02
94. Tribufos (+merphos) 19.06
95. Oxyfluorfen 19.14
96. Dieldrin 19.16
97. 2,3,3',4',6-Pentachlorobiphenyl 19.18
98. Nitrofen 19.59
99. Endrin 19.67
100. 2,2',3,4',5',6-Hexachlorobiphenyl 19.74
101. Chlorobenzilate 19.81
102. 2,3',4,4',5-Pentachlorobiphenyl 19.83
103. Endosulfan II 19.91
104. 4,4'-DDD 20.02
105. Ethion 20.02
106. 2,2',4,4',5,5'-Hexachlorobiphenyl 20.35
107. Norflurazon 20.68
108. Butylbenzylphthalate 20.82
109. Endosulfan sulfate 20.85
110. 4,4'-DDT 20.96
111. 2,2',3,4,4',5'-Hexachlorobiphenyl 20.99
112. Hexazinone 21.04
113. Tebuconazole 21.27
114. Di(2-ethylhexyl)adipate 21.29
115. Triphenyl phosphate (SS) 21.38
116. Benzo[a]anthracene 22.19
117. Chrysene-D12 (IS) 22.22
118. Chrysene 22.30
119. Methoxychlor 22.32
120. 2,2',3,4,4',5,5'-Heptachlorobiphenyl 22.62
121. Di(2-ethylhexyl)phthalate 22.84
122. Fenarimol 23.72
123. cis- Permethrin24.57
124. trans- Permethrin24.75
125. Benzo[b]fluoranthene 25.44
126. Benzo[k]fluoranthene 25.53
127. Benzo[a]pyrene-D12 (SS) 26.27
128. Benzo[a]pyrene 26.33
129. Fluridone 26.46
130. Indeno[1,2,3-cd]pyrene 29.24
131. Dibenzo[a,h]anthracene 29.34
132. Benzo[g,h,i]perylene 29.84
GC_EV1436
Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) EPA Method 525.3 OCP cal standard (cat.# 32542) EPA Method 525.3 OPP cal standard (cat.# 32543) EPA Method 525.3 ONP cal standard (cat.# 32544) EPA Method 525.3 PAH cal standard (cat.# 32545) EPA Method 525.3 PCB cal standard (cat.# 32546) EPA Method 525.3 PAH IS mix (cat.# 32547) EPA Method 525.3 PCP IS (cat.# 32548) EPA Method 525.3 surrogate standard (cat.# 32549)
Ethyl acetate 2 µg/mL (Pentachlorophenol concentration: 8 µg/mL) 1 µL pulsed splitless (hold 1 min) Premium 4 mm single taper w/wool (cat.# 23303.1) 275 °C 30 psi (206.8kPa) 1 min 80 mL/min 70 °C (hold 1 min) to 200 °C at 10 °C/min to 320 °C at 7 °C/min (hold 3 min) He, constant flow 1.2 mL/min MS Scan Group Start Time (min) Scan Range (amu) Scan Rate (scans/sec) 1 5 45-550 5.5
280 °C Quadrupole Extractor 6 mm ID 350 °C 200 °C 5 min DFTPP EI Agilent 7890B GC & 5977A MSD
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