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Bergamot Oil on Rxi-5Sil MS

PeakstR (min)
1.α-Thujene2.005
2.α-Pinene2.067
3.Sabinene2.233
4.β-Myrcene2.253
5.β-Pinene2.296
6.p-Cymene2.516
7.D-Limonene2.553
8.3-Carene2.585
9.γ-Terpinene2.724
10.Terpinolene2.926
PeakstR (min)
11.Linalool2.963
12.α-Terpineol3.841
13.Z-Citral4.191
14.Bergamol4.276
15.E-Citral4.462
16.2-Carene5.310
17.Neryl acetate5.353
18.Geranyl acetate5.557
19.Caryophyllene6.212
20.α-Bergamotene6.266
21.β-Bisabolene7.034
image
GC_FF1309
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
SampleBergamot oil
Diluent:Acetone
Conc.:5%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 300 °C at 11 °C/min (hold 10 min)
Carrier GasHe, constant flow
Flow Rate:1.31 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
11.0035-5005
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Type:Inert
Source Temp.:230 °C
Quad Temp.:150 °C
InstrumentAgilent 7890A GC & 5975C MSD
NotesAll peaks were identified using the NIST MS EI spectra library (2005).
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