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Organophosphorus Pesticides in AOAC QuEChERS Solvent on Rxi-5ms

GC_FS0541
Column | Rxi-5ms, 15 m, 0.25 mm ID, 0.25 µm (cat.# 13420) |
Sample | 8140/8141 OP pesticide calibration mix A (cat.# 32277) |
Diluent: | 1% Acetic acid in acetonitrile |
Conc.: | 1 ng/µL |
Injection | |
Inj. Vol.: | 1 µL splitless (hold 1.5 min) |
Liner: | Premium 4 mm single taper w/wool (cat.# 23303.1) |
Inj. Temp.: | 250 °C |
Purge Flow: | 40 mL/min |
Oven | |
Oven Temp.: | 70 °C (hold 1.5 min) to 330 °C at 12.7 °C/min (hold 3.0 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1 mL/min |
Detector | FID @ 350 °C |
Constant Column + Constant Make-up: | 50 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 10 Hz |
Instrument | Agilent/HP6890 GC |
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