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GC Multiresidue Pesticide Standard #1-OPP on Rxi-5ms by GC-MS

PeakstR (min)
1.Diazinon13.97
2.Isazophos14.27
3.Chlorpyrifos methyl15.07
4.Fenitrothion15.72
5.Pirimiphos methyl15.76
6.Chlorpyrifos16.21
7.Pirimiphos ethyl16.71
8.Quinalphos17.21
PeakstR (min)
9.Pyridaphenthion20.99
10.Phosmet21.06
11.EPN21.14
12.Phosalone21.89
13.Azinphos methyl21.90
14.Pyrazophos22.58
15.Azinphos ethyl22.63
16.Pyraclofos22.73
image
GC_FS0600
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleGC multiresidue pesticide standard #1-OPP (cat.# 32563)
Diluent:Toluene
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4.0 mm ID Precision inlet liner w/wool (cat.# 23305.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1555-5507
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Electron Energy:70 eV
Solvent Delay Time:5 min
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesReconstructed chromatogram from select ions.
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