Biodiesel Oil on Rtx-Biodiesel TG

ColumnRtx-Biodiesel TG, 10 m, 0.32 mm ID, 0.10 µm (cat.# 10292)
SampleB100 biodiesel oil plus butanetriol and tricaprin, in heptane, derivatized with MSTFA
Inj. Vol.:1 µL on-column
Inj. Temp.:oven track
Oven Temp.:50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 370 °C at 10 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:4 mL/min
DetectorFID @ 390 °C
InstrumentShimadzu 2010 GC
NotesInjection onto Shimadzu on-column injector (OCI) equipped with low dead volume Shimadzu direct injection liner
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