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Derivatized B100 and Internal Standards on MXT-Biodiesel TG with 2 m Integra Gap

GC_PC00934
Column | MXT-Biodiesel TG 13 m, 0.53 mm ID, 0.16 µm with built-in 2 m Integra-Gap (total column length 15 m) |
Sample | B100 + IS butanetriol & tricaprin derivatized with MSTFA as per ASTM D-6584 |
Injection | |
Inj. Vol.: | 1.0 µL cold on-column |
Temp. Program: | oven track |
Oven | |
Oven Temp.: | 50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 430 °C at 30 °C/min (hold 5 min) |
Carrier Gas | H2, constant flow |
Flow Rate: | 4 mL/min |
Detector | FID @ 430 °C |
Instrument | Shimadzu 2010 GC |
Notes | (Data acquired on prototype column, similar column to cat# 70290) |
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total glycerides
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