This chromatogram may contain analytes that are synonyms of your search terms.

Dynamic Headspace USP <467> solvents on Rtx-1301 (G43)

PeakstR (min)sample concentration (µg/ml)
ColumnRtx-1301 (G43), 30 m, 0.53 mm ID, 3.00 µm (cat.# 16085-126)
SampleUSP <467> Calibration Mixture #5 (cat.# 36007)
Diluent:DMSO stock standard
Conc.: To each 22mL headspace vial 5ml water, ~ 1.0g of sodium sulfate and 100µL of stock standard were added. The preparations yielded the concentrations above.
Injectionheadspace-trap split
Oven Temp.:40 °C (hold 20 min) to 240 °C at 25 °C/min (hold 10 min)
Carrier GasHe, constant flow
Flow Rate:5 mL/min
DetectorFID @ 250 °C
Make-up Gas Flow Rate:45 mL/min
Hydrogen flow: 40 mL/min
Air flow: 450 mL/min

Dynamic Headspace (Trap) Conditions:
Instrument: Teledyne Tekmar HT3
Valve oven temp.: 150°C
Transfer line temp.: 150°C
Standby flow rate: 10mL/min.
Trap standby temp.: 40°C
Platen/sample temp.: 80°C
Sample equil. time: 15.00 min.
Mixer time: 2.00 min.
Mixing level: 5
Mixer stabilize time: 0.50 min.
Sweep flow rate: 75mL/min.
Sweep flow time: 3.00 min.
Dry purge time: 5.00 min.
Dry purge flow: 50mL/min.
Dry purge temp.: 25°C
Desorb preheat: 245°C
Desorb temp.: 250°C
Desorb time: 1.00 min.
Trap bake temp.: 300°C
Trap bake time: 6.00 min.
Trap bake flow: 450mL/min.
Download PDF

Printing tips! To print chromatograms full page, change the print settings in the print dialogue window of your PDF reader software: 1) "fit" or "fit to page", 2) "landscape" for wide chromatograms or "portrait" for tall chromatograms.

Restek Domestic Customer Service



Your Full Name

Your Email

Company Name


Spam Block (Please leave this blank)

all fields required

Thank you

Your message has been sent. We will be in touch shortly.

Message not sent

Sorry, your message could not be sent at this time. Please try again later, or contact Restek or your local Restek representative via phone.