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This chromatogram may contain analytes that are synonyms of your search terms.

Residual Solvents Class 2 Mixture A on Rtx-624

Peaks
1.Methanol
2.Acetonitrile
3.Dichloromethane
4.trans-1,2-Dichloroethene
5.cis-1,2-Dichloroethene
6.Tetrahydrofuran
7.Cyclohexane
Peaks
8.Methylcyclohexane
9.1,4-Dioxane
10.Toluene
11.Chlorobenzene
12.Ethyl benzene
13.m-Xylene/ p-Xylene
14.o-Xylene
image
GC_PH00910
ColumnRtx-624, 30 m, 0.32 mm ID, 1.80 µm (cat.# 10970)
SampleResidual Solvents Class 2 - Mix A (cat.# 36271)
in 20 mL headspace vial
Injectionheadspace-loop split (split ratio 5:1)
Liner:Siltek 1mm Split
Headspace-Loop
Inj. Port Temp.:140 °C
Instrument:Tekmar HT3
Inj. Time:1.00 min
Transfer Line Temp.:105 °C
Valve Oven Temp.:105 °C
Sample Temp.:80 °C
Sample Equil. Time:45 min
Vial Pressure:10 psi
Pressurize Time:0.5 min
Loop Pressure:5 psi
Loop Fill Time:2.00 min
Oven
Oven Temp.:40 °C (hold 20 min) to 240 °C at 10 °C/min (hold 20 min)
Carrier GasHe, constant flow
Flow Rate:2.16 mL/min
Linear Velocity:35.3 cm/sec
DetectorFID @ 240 °C
NotesSiltek 1mm Split obsolete, recommend catalog number 20972
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