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Alkyl Halide Genotoxic Impurities on Rxi-624Sil MS (High Concentration Injection)
Peaks | tR (min) | |
---|---|---|
1. | 2-Chloropropane![]() | 2.10 |
2. | Bromoethane![]() | 2.36 |
3. | 1-Chloropropane![]() | 2.72 |
4. | 2-Bromopropane![]() | 3.393 |
5. | Butyl chloride![]() | 4.627 |
6. | 1-Bromobutane![]() | 5.973 |

GC_PH1166
Column | Rxi-624Sil MS, 20 m, 0.18 mm ID, 1.00 µm (cat.# 13865) |
Sample | |
Diluent: | DMSO |
Conc.: | 1 µg/mL |
Injection | |
Inj. Vol.: | 1 µL splitless (hold 0.5 min) |
Liner: | 3.5 mm Single Gooseneck Liner with wool placed 3 cm from top (middle) (cat.# 22286) |
Inj. Temp.: | 220 °C |
Purge Flow: | 3 mL/min |
Oven | |
Oven Temp.: | 40 °C (hold 3 min) to 200 °C at 20 °C/min |
Carrier Gas | He, constant flow |
Linear Velocity: | 40 cm/sec |
Detector | MS |
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Analyzer Type: | Quadrupole |
Source Temp.: | 280 °C |
Solvent Delay Time: | 0.5 min |
Ionization Mode: | EI |
Scan Range: | 30-300 amu |
Scan Rate: | 5 scans/sec |
Instrument | Shimadzu 2010 GC & QP2010+ MS |
Notes | Ions displayed: 42, 43, 57, 108 m/z |
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