Analysis of Mycotoxins on Raptor FluoroPhenyl by LC-MS/MS

	Peaks	tR (min)	Conc. (ng/mL)	Precursor Ion	Product Ion	Product Ion
1.	Nivalenol	1.04	100	313.22	175.09	91.08
2.	Patulin	1.42	50	155.00	98.94	80.98
3.	Deoxynivalenol	1.53	50	297.20	249.04	231.03
4.	Fusarenon X	2.13	100	355.20	247.10	175.08
5.	15-Acetyldeoxynivalenol	3.07	100	339.23	321.15	137.07
6.	3-Acetyldeoxynivalenol	3.22	100	339.16	231.10	213.08
7.	Aflatoxin M1	4.11	25	329.22	273.09	229.12
8.	Diacetoxyscirpenol	4.41	100	367.24	307.14	105.07
9.	Aflatoxin G2	4.67	25	331.16	313.00	189.01
10.	Aflatoxin G1	4.87	25	329.13	243.00	199.74
11.	HT-2	4.92	50	447.20	345.08	285.11
12.	Aflatoxin B2	5.20	25	315.13	287.02	258.98
13.	Aflatoxin B1	5.32	25	313.16	284.85	241.06
14.	Citrinin	5.38	10	251.15	233.09	205.05
15.	Fumonisin B1	5.56	25	722.46	352.25	334.23
16.	T-2	5.63	50	489.24	245.07	387.12
17.	Fumonisin B3	6.03	25	706.43	336.23	318.29
18.	Ochratoxin A	6.17	25	404.07	238.96	357.98
19.	Fumonisin B2	6.31	25	706.43	336.23	318.29
20.	Zearalenone	6.44	50	319.23	283.06	187.04

LC_FS0511

Column	Raptor FluoroPhenyl (cat.# 9319A12)
Dimensions:	100 mm x 2.1 mm ID
Particle Size:	2.7 µm
Pore Size:	90 Å
Guard Column:	Raptor FluoroPhenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9319A0252)
Temp.:	30 °C
Sample
Diluent:	Water:methanol (80:20)
Conc.:	10-100 ng/mL
Inj. Vol.:	5 µL
Mobile Phase
A:	0.3% Formic acid in water
B:	Methanol
	Time (min) Flow (mL/min) %A %B 0.00 0.4 80 20 7.00 0.4 10 90 7.01 0.4 80 20 9.00 0.4 80 20
Max Pressure:	525 bar
Detector	MS/MS
Ion Mode:	ESI+
Mode:	MRM
Instrument	UHPLC

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Raptor FluoroPhenyl

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FluoroPhenyl

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