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Cannabis Mycotoxins in Solvent on Raptor Biphenyl by LC-MS/MS

PeakstR (min)Precursor IonProduct Ion 1Product Ion 2
1.Aflatoxin G21.342331.2189.3115.2
2.Aflatoxin G11.578329.2243.2215.3
3.Aflatoxin B21.706315.3287.2243.3
4.Ochratoxin A1.818404.3239.1358.3
5.Aflatoxin B11.943313.2241.2128.2
image
LC_GN0583
ColumnRaptor Biphenyl (cat.# 9309A52)
Dimensions:50 mm x 2.1 mm ID
Particle Size:2.7 µm
Pore Size:90 Å
Guard Column:Raptor Biphenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9309A0252)
Temp.:35 °C
Sample
Diluent:45:55 Water:Methanol
Conc.:50 ng/mL
Inj. Vol.:5 µL
Mobile Phase
A:Water, 2 mM ammonium formate, 0.1% formic acid
B:Methanol, 2 mM ammonium formate, 0.1% formic acid
Time (min)Flow (mL/min)%A%B
0.000.73565
2.000.71090
2.010.73565
3.000.73565
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentUHPLC
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mycotoxins

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