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Long-Life ESI Electrode

..., Instrument, Sciex Turbo V Ion Sources, Model #, API 3200, 3500, 4000, 4500, 5000, 5500+, 6500 ... API 3200, 3500, 4000, 4500, 5000, 5500+, 6500, and 6500+...

Two Options for Analyzing Potential Genotoxic Impurities in Active Pharmaceutical Ingredients

... Laboratory needs for analyzing PGIs in API vary. Here we developed both a fast of active pharmaceutical ingredients (API), or reaction byproducts that form during synthesis, have ... Two options for the analysis of PGIs in API have been developed by Merck and Restek to meet ... PGI, sulfonate ester, potential genotoxic impurities, rtx-200, API, Rxi-5Sil MS...

ChromaBLOGraphy: GC-API-MS for BDEs with N2 at BFR2016

OK Jack, enough of the acronyms; this isn’t a word puzzle… Recently I let ChromaBLOGraphy readers know of our work on using gas chromatography (GC) with atmospheric pressure ionization (API) – mass spectrometry (MS) for analysis of brominated diphenyl ethers (BDEs) employing nitrogen (N2) carrier gas, which was presented at BFR2016 (BFR standing for Brominated […]

Analysis of Synthetic Cannabinoids and Metabolites: Adding New Compounds to an Existing LC-MS/MS Method (PDF 870kB)

... with a SCIEX API 4500 MS/MS. Both systems utilized electrospray ionization in positive ion mode using scheduled .3/144.2 Detector AB SCIEX API 4000 MS/MS Model #: API 4000 Ion Source: TurboIonSpray Ion Mode: ESI+ Ion Spray...

4.5 Minute Analysis of Benzodiazepines in Urine and Whole Blood Using LC/MS/MS and an Ultra Biphenyl Column (PDF 672kB)

.../mL. This method, which uses an Ultra Biphenyl LC column and an API 4000 MS/MS detector, provides a fast 4.5 minute using a Shimadzu UFLCXR HPLC coupled with an AB SCIEX® API 4000 MS/MS operating in positive electrospray...

Raptor Biphenyl LC Columns Brochure (PDF 6071kB)

....6 mL/min Detector: AB SCIEX API 4000 MS/MS Ion Source: TurboIonSpray Ion Mode: ESI+ Instrument : API LC-MS/MS Notes: Lorazepam was prepared at 100 ng/mL; all other analytes are 10 ng/mL. Peaks t...

Get More Uptime with Restek’s Long-Life ESI Electrode for Sciex Turbo V Sources (PDF 1130kB)

... Sample Pos PPG 1x10-5 M Conc.: 1x10-5 Molar Mobile Phase Flow: mL/min Detector API 4000 Ion Source .: 1x10-5 Molar Mobile Phase Flow: mL/min Detector API 4000 Ion Source: Electrospray Ion Mode: ESI...

Raptor Biphenyl LC Columns Sales Sheet (PDF 3731kB)

...%); Flow: 0.6 mL/min; Detector: AB SCIEX API 4000 MS/MS; Ion Source: TurboIonSpray; Ion Mode: ESI +; Instrument: API LC-MS/MS; Notes: Lorazepam was prepared at 100 ng/mL; all other analytes are 10 ng/mL. Peaks...

A Comprehensive Approach to Pesticide Residue Monitoring, Including Non-target Analysis, for Fruits, Vegetables, and Nuts, Using QuEChERS, LC-MS/MS, and GCxGC-TOFMS (PDF 2552kB)

... with gradient program; Flow: 0.5 mL/min; Detector: AB SCIEX API 4000 LC/MS/MS System; Ion Source: Turbo IonSpray; Ion Mode: ESI+; Mode: MRM; Instrument: API LC-MS/MS. Figure 6: Contour plot region for elution area...

Overcoming the Effects of Highly Organic Protein Precipitation Extracts on LC Peak Shape Using Direct Injection (PDF 585kB)

... and undiluted extracts) were analyzed using a Shimadzu Nexera UHPLC equipped with a SCIEX API 4500 MS/MS under...

Rapid Analysis of C3 Epimers of 25-Hydroxyvitamin D in Serum by LC-MS/MS (PDF 559kB)

...L) for analysis. LC analysis was performed on a Shimadzu Nexera XR LC coupled with a Sciex API 4000 mass...

Direct Analysis of Morphine, M3G and M6G Metabolites, and Related Compounds in Urine by LC-MS/MS (PDF 778kB)

... compounds was conducted on a Shimadzu Nexera UHPLC equipped with a SCIEX API 4500 MS/MS. Detection...

Raptor ARC-18 LC Columns Brochure (PDF 4942kB)

...%), 7.0 (90%); Flow: 0.5 mL/min; Detector: AB SCIEX API 4000; Ion Source: TurboIonSpray; Ion Mode: ESI...

Analysis of Amphetamines by LC-MS/MS for High-Throughput Urine Drug Testing Labs (PDF 1198kB)

...-MS/MS was performed on a Shimadzu Prominence HPLC equipped with a SCIEX API 4000 MS/ MS. Instrument conditions were...

Mitigating Matrix Effects: Examination of Dilution, QuEChERS, and Calibration Strategies for LC-MS/MS Analysis of Pesticide Residues in Diverse Food Types (PDF 1561kB)

... A Shimadzu UFLCXR LC (Columbia, MD) and Applied Biosystems/MDS SCIEX AB SCIEX API 4000 LC-MS/MS system .5 90 10 15.00 0.5 90 10 Detector ABSCIEX MS/MS Model #: API 4000 Ion Source: TurboIonSpray Ion...

Introduction Ethyl glucuronide (EtG) and ethyl sulfate (EtS) are important... (PDF 1212kB)

... that require lower detection limits or labs using legacy instruments (e.g., SCIEX API 4000) that may not have...

ChromaBLOGraphy: SWAFS: Chromatography of Beer & Urine.

This year Keith Irwin will be attending the Southwest Association of Forensic Scientists (SWAFS) the first week of October to give a presentation on Bath Salts, Synthetic Cannabinoids and he plans on handing out a few cold ones. How does the Innovations laboratory fit into this picture?  First Amanda Rigdon put together over a year’s [...]

Restek LC Columns and Accessories (PDF 17409kB)

....10 min (5%), 7.00 min (5%); Flow: 0.6 mL/min; Detector: AB SCIEX API 4000 MS/MS; Ion Source: Turbo IonSpray; Ion Mode: ESI+; Instrument: API LC-MS/MS; Notes: Lorazepam was prepared at 100 ng/mL; all other...

One Stop Shop for EPA Method 535 Reliably Analyze Acetamide Herbicide Degradates by LC/MS/MS

... on an Ultra C18 column coupled to an Applied Biosystems API 3200 LC/MS/MS system equipped with a Turbo...

Analysis of Synthetic Cannabinoids and Metabolites: Adding New Compounds to an Existing LC-MS/MS Method

... I-Class equipped with a Xevo TQ-S and a Shimadzu Nexera UHPLC equipped with a SCIEX API 4500 MS...

4.5 Minute Analysis of Benzodiazepines in Urine and Whole Blood Using LC/MS/MS and an Ultra Biphenyl Column

... 0.5 ng/mL to 10 ng/mL. This method, which uses an Ultra Biphenyl LC column and an API 4000 MS in triplicate using a Shimadzu UFLCXR HPLC coupled with an AB SCIEX® API 4000 MS...

Rapid Analysis of C3 Epimers of 25-Hydroxyvitamin D in Serum by LC-MS/MS

... Nexera XR LC coupled with a Sciex API 4000 mass spectrometer. Instrument conditions were as follows...

Overcoming the Effects of Highly Organic Protein Precipitation Extracts on LC Peak Shape Using Direct Injection

... with a SCIEX API 4500 MS/MS under the conditions shown below. The analyte transitions that were monitored...

Direct Analysis of Morphine, M3G and M6G Metabolites, and Related Compounds in Urine by LC-MS/MS

... UHPLC equipped with a SCIEX API 4500 MS/MS. Detection was performed using electrospray ionization...

Analysis of Amphetamines by LC-MS/MS for High-Throughput Urine Drug Testing Labs

... Analysis of amphetamines by LC-MS/MS was performed on a Shimadzu Prominence HPLC equipped with a SCIEX API...

Successful Strategies for the Analysis of EtG and EtS in Urine Rugged Sample Preparation and Analysis Conditions for High-Throughput Labs

...require lower detection limits or labs using legacy instruments (e.g., SCIEX API 4000) that may n...

Mitigating Matrix Effects: Examination of Dilution, QuEChERS, and Calibration Strategies for LC-MS/MS Analysis of Pesticide Residues in Diverse Food Types

... Biosystems/MDS SCIEX AB SCIEX API 4000 LC-MS/MS system with Turbo V source (Foster City, CA) were used for LC...

For advanced chromatogram searching, please check out our Chromatogram Library Search Tool.

Antipsychotics and Antidepressants in Human Urine on Raptor Biphenyl by LC-MS/MS

LC_CF0749

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Butter Triglycerides on Rtx-65TG

GC_FF00137

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PEGylated Oxytocin on Viva C18

LC_PH0467

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Carbamates on Ultra Carbamate

LC_FF0473

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